NMR Restraints Grid |
Result table
image | mrblock_id | pdb_id | bmrb_id | cing | stage | program | type |
1619 | 1arr | 395 | cing | 1-original | MR format | comment |
*HEADER GENE-REGULATING PROTEIN 24-AUG-93 1ARR *COMPND ARC REPRESSOR (NMR, MINIMIZED AVERAGE STRUCTURE) *SOURCE SALMONELLA BACTERIOPHAGE P22 *AUTHOR A.M.J.J.BONVIN,H.VIS,M.J.M.BURGERING,J.N.BREG,R.BOELENS, *AUTHOR 2 R.KAPTEIN *REVDAT 1 31-JAN-94 1ARR 0 REMARK 3 NOE build-ups were obtained from NOESY spectra recorded REMARK 3 at 600 MHz in H2O and D2O. Additional constraints were REMARK 3 obtained from a SCUBA experiment revealing NOEs close to REMARK 3 the water frequency and from 3D (15N,1H) heteronuclear REMARK 3 experiments (3D NOE-HMQC). REMARK 3 The total number of constraints was 1002 per monomer. REMARK 3 These consisted of 350 intraresidue, 215 sequential, REMARK 3 223 medium-range and 214 long range constraints; 150 REMARK 3 of the total set correspond to intermonomer constraints. REMARK 3 16 methylene proton pairs and the methyl groups of 4 valine REMARK 3 residues could be stereospecifically assigned. From the REAMRK 3 stereospecific assignment procedure 21 chi-1 dihedral angle REMARK 3 constraints could be imposed. REMARK 5 Arc experimental NOE build-ups (1064) in H2O at 600 MHz REMARK 5 The three mixing times are: 0.10000 0.15000 0.20000 [s] REMARK 5 Methyl groups are indicated by Q3###. The stereospecifically REMARK 5 assigned protons are listed below. For peaks involving REMARK 5 diastereotopic protons that were not stereospecifically REMARK 5 assigned an arbitrary assignment is given. REMARK 5
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